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Quantification of benzoxazinoids and their metabolites in Nordic breads.

Katharina Dihm (Institutionen för biologi och bioteknik, Livsmedelsvetenskap ; Institutionen för kemi och kemiteknik, Organisk kemi) ; Mads Vendelbo Lind (Institutionen för biologi och bioteknik, Livsmedelsvetenskap) ; Henrik Sundén (Institutionen för kemi och kemiteknik, Organisk kemi) ; Alastair Ross (Institutionen för biologi och bioteknik, Livsmedelsvetenskap) ; Otto Savolainen (Institutionen för biologi och bioteknik, Livsmedelsvetenskap)
Food chemistry (0308-8146). Vol. 235 (2017), p. 7-13.
[Artikel, refereegranskad vetenskaplig]

Benzoxazinoids (Bx) and their metabolites are molecules with suggested health effects in humans, found in cereal grains and consequently in cereal foods. However, to date little is known about the amount of Bx in our diet. In this study, deuterated standards 2-hydroxy-1,4-benzoxazin-3-one (HBOA-d4) and 2-hydroxy-N-(2-hydroxyphenyl) acetamide (HHPAA-d4) were synthesized, to allow quantification of nine Bx and their metabolites in 30 breads and flours from Nordic countries by UHPLC-MS/MS. Samples containing rye had larger amounts of Bx (143-3560µg/g DM) than the ones containing wheat (11-449µg/g DM). More Bx were found in whole grain wheat (57-449µg/g DM) compared to refined wheat (11-92µg/g DM) breads. Finnish sourdough rye breads were notably high in their 2-hydroxy-N-(2-hydroxyphenyl) acetamide (HHPAA) concentration (40-48µg/g DM). This new information on Bx content in flours and breads available in the Nordic countries will be useful for future work on determining dietary exposure to Bx.

Nyckelord: Benzoxazines, analysis, Bread, analysis, Finland, Humans, Secale, Tandem Mass Spectrometry, Triticum

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Denna post skapades 2017-08-25. Senast ändrad 2017-09-14.
CPL Pubid: 251414


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