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Reduction of multiple hits in atom probe tomography

Mattias Thuvander (Institutionen för teknisk fysik, Materialens mikrostruktur ) ; Anders Kvist (Institutionen för teknisk fysik, Materialens mikrostruktur ) ; Lars J S Johnson ; Jonathan Weidow (Institutionen för teknisk fysik, Materialens mikrostruktur ) ; Hans-Olof Andrén (Institutionen för teknisk fysik, Materialens mikrostruktur )
Ultramicroscopy (0304-3991). Vol. 132 (2013), p. 81-85.
[Artikel, refereegranskad vetenskaplig]

The accuracy of compositional measurements using atom probe tomography is often reduced because some ions are not recorded when several ions hit the detector in close proximity to each other and within a very short time span. In some cases, for example in analysis of carbides, the multiple hits result in a preferential loss of certain elements, namely those elements that frequently field evaporate in bursts or as dissociating molecules. In this paper a method of reducing the effect of multiple hits is explored. A fine metal grid was mounted a few millimeters behind the local electrode, effectively functioning as a filter. This resulted in a decrease in the overall detection efficiency, from 37% to about 5%, but also in a decrease in the fraction of multiple hits. In an analysis of tungsten carbide the fraction of ions originating from multiple hits decreased from 46% to 10%. As a result, the measured carbon concentration increased from 48.2 at%to 49.8 at%, very close to the expected 50.0 at%. The character- istics of the multiple hits were compared for analyses with and without the grid filter.

Nyckelord: Atom probe tomography, Multiple hits, Detection efficiency, Quantification, Carbides, Tungsten carbide



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Denna post skapades 2013-10-07. Senast ändrad 2015-03-30.
CPL Pubid: 184855

 

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Institutioner (Chalmers)

Institutionen för teknisk fysik, Materialens mikrostruktur (2012-2015)

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