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The preparation of a solubilized form of Lawessons reagent and its thionation reactions

Mark Foreman (Institutionen för kärnkemi) ; A. M. Z. Slawin ; J. D. Woollins
Heteroatom Chemistry (1042-7163). Vol. 10 (1999), 7, p. 651-657.
[Artikel, refereegranskad vetenskaplig]

2-tert-Butylanisole and P4S10 react together to give 2,4-bis (3-tbutyl-4-methoxyphenyl) 1,3, 2, 4-dithiadiphosphetane 2, 4-disulfide (LR*) which was characterized by X-ray crystallography. Comparative thionation reactions of LR* and a range of P-S compounds were investigated. If was found that LR* in many cases, gives better yields of thionated complexes than Lawessons Reagent when the reactions are performed at room temperature. (C) 1999 John Wiley & Sons, Inc.

Denna post skapades 2013-05-22. Senast ändrad 2015-07-28.
CPL Pubid: 177197


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